The Chemistry of Dinitrogen Residues. Part 3. Hydrazido(2-)-derivatives of Titanium(IV). X-Ray Crystal Structure of 2>

DOI: 10.1039/DT9860000393

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Journal of the Chemical Society, Dalton Transactions p. 393 - 398 (1986)

Update date:2022-07-30

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Authors:

Hughes, David L.

Latham, Ian A.

Leigh, G. Jeffery

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Article abstract of DOI:10.1039/DT9860000393

The preparations of 1,2-hydrazide(2-) and 1,1-hydrazide(2-) complexes of titanium(IV) are described.The 1H n.m.r. spectra of dinuclear 1,1-disubstituted hydrazide(2-) complexes, such as <2>, are anomalous, but can be explained on the basis of an X-ray structure analysis which shows that one hydrazide forms a symmetrical bridge whereas the other is both bridging and bound side-on to one of the titaniums.

Full text of DOI:10.1039/DT9860000393

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