Tetrahedron p. 4235 - 4246 (1986)
Update date:2022-07-30
Topics:
Baldwin, Jack E.
Adlington, Robert M.
Bottaro, Jeffrey C.
Kolhe, Jayant N.
Newington, Ian M.
Perry, Matthew W. D.
The lithium salts of trityl- and diphenyl-4-pyridylmethyl-hydrazones of both aldehydes and ketones react with electrophiles (alkyl halides, aldehydes, ketones, crotonates) at low temperature to form C-trapped azo compounds; these intermediates decompose homolytically with loss of nitrogen below room temperature and can be diverted in a synthetically useful way to alkanes, alkenes, alcohols or saturated esters.
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(2015)Doi:10.1021/jm00162a008
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(1986)Doi:10.1002/jhet.5570230209
(1986)Doi:10.1002/anie.201301529
(2013)Doi:10.1002/anie.200903387
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