Tetrahedron Letters p. 845 - 846 (1986)
Update date:2022-09-26
Topics:
Ferroud, D.
Gaudin, J. M.
Genet, J. P.
(E)-9-oxo-2-decenoic acid (queen substance) (1); (E)-3,7-dimethyl-2,7-octadienyl propionate (2) and (E)-3,7-dimethyl-2-octene-1,8-diol (3) are easily synthesized via sequential alkylation of bis-(arylsulfonyl)methane 4 with 1,4-allylic substrates 7 and a second electrophile such as 4,4-(ethylenedioxy)pentyl iodide and ethyl 2-methylallyl carbonate.
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