SYNTHESIS OF 1,4-DIDEOXY-1,4-IMINO-D-GLUCITOL, A GLUCOSIDASE INHIBITOR

Article abstract of DOI:10.1016/S0008-6215(00)90194-0

1,2:5,6-Di-O-isopropylidene-D-glucitol was converted via its 1,4-dimethanesulfonate into the 1-azido-4-methanesulfonate which, after deprotection and treatment with barium hydroxide, afforded a 9:1 mixture of the corresponding 3,4- and 4,5-anhydro derivat