Journal of Organic Chemistry p. 27 - 30 (1988)
Update date:2022-08-03
Topics:
Hassner, Alfred
Amarasekara, Ananda S.
Andisik, Donald
A facile synthetic route from aldehydes to allyl α-azidoalkyl ether 2 is described.Thermolysis of 2 proceeds by intramolecular azide-olefin cycloaddition via triazolines and provides a novel synthesis of 2,5-dihydrooxazoles 6.The use of silica gel in the chemoselective conversion of the intermediate triazolines to bicyclic aziridines 7 is described.
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