Journal of the Chemical Society, Dalton Transactions p. 2503 - 2504 (1987)
Update date:2022-08-04
Topics:
McCullough, Kevin J.
Bladon, Peter
Janecki, Tomasz
Pauson, Peter
N-Benzylacetimidic acid ethyl ester (L) yields a stable complex of the type trans-a centrosymmetric structure a=9.983(4), b=9.492(23), c=14.111(10) Angstroem, β=114.02(4) deg, and Z=2>.Splitting of the (1)H n.m.r. signal corresponding to the CH3C=group is attributed to the presence of two slowly interconverting rotamers (probably about the Pd-N bond), while a more rapid fluxional mode must be responsible for the temperature variation in the chemical shift of the CH2O groups.
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Doi:10.1039/P19870001165
(1987)Doi:10.1021/ol8028324
(2009)Doi:10.1016/S0040-4039(00)85440-4
(1986)Doi:10.1021/ol8028687
(2009)Doi:10.1055/s-1987-27998
(1987)Doi:10.1016/S0040-4039(00)95768-X
(1987)
