Journal of Organometallic Chemistry p. 115 - 124 (1987)
Update date:2022-08-05
Topics:
Caygill, Graham B.
Steel, Peter J.
Six pyrazoles have been cyclopalladated by reaction with either lithium tetrachloropalladate or palladium acetate and the dimeric products converted to monomeric acetylacetonate complexes.The crystal structure of acetylacetonato<2-(3-methyl-5-phenylpyrazol-1-yl)phenyl-C1,N2'>palladium(II) has been determined.Crystals are monoclinic: a 15.035(3), b 8.541(1), c 16.340(4) Angstroem, β 117.10(1) deg, P21/c, Z = 4; the structure was refined to R = 0.030.
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