A simple method of regenerating areneruthenium dichloride dimers, 6-arene)>2, from their monomeric adducts with amines or tertiary phosphines, RuCl2(η6-arene)L

DOI: 10.1016/0022-328X(88)80645-4

Source and publish data:

Journal of Organometallic Chemistry p. 117 - 122 (1988)

Update date:2022-08-02

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Authors:

Pertici, Paolo

Bertozzi, Sergio

Lazzaroni, Raffaello

Vitulli, Giovanni

Bennett, Martin A.

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Article abstract of DOI:10.1016/0022-328X(88)80645-4

The monomeric amine or tertiary phosphine complexes RuCl2(η⁶-arene)L (arene=benzene, p-cymen) can be reconverted into their dimeric precursors 6-arene)>2 by heating with 1,5-cyclooctadiene (COD), 2-propanol, and anhydrous Na2CO3 and subsequent treatment of the resulting ruthenium(0) complexes Ru(η⁶-arene)(η⁴-COD) with HCl; the ligand L can be recovered.

Full text of DOI:10.1016/0022-328X(88)80645-4

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