One-Pot Synthesis of 4,5-Unsubstituted 1,3-Dithioles and 2-Alkylidene-1,3-dithioles from 1,3-Dithiolane S-Oxides

DOI: 10.1055/s-1990-26849

Source and publish data:

Synthesis p. 271 - 273 (1990)

Update date:2022-07-30

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Authors:

Schaumann, Ernst

Winter-Extra, Susanne

Kummert, Knut

Scheiblich, Stefan

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Article abstract of DOI:10.1055/s-1990-26849

An efficient synthesis of the title compounds via formal dehydration of the corresponding 1,3-dithiolane S-oxides with iodotrimethylsilane and diisopropylethylamine (Huenig's base) is reported.

Full text of DOI:10.1055/s-1990-26849

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