Journal of Organic Chemistry p. 2534 - 2538 (1991)
Update date:2022-08-03
Topics:
Linde, Robert G.
Jeroncic, Lucio O.
Danishefsky, Samuel J.
A simple two-step protocol for the preparation of α,β-diketo amides is described.The first step involves condensation of the anion of an α-phenylthio amide with an aldehyde.This is followed by oxidation of the resulting β-hydroxy α-sulfide with the Dess-Martin periodinane.The vicinal tricarbonyl system is obtained in good to excellent yields.
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