Synthesis p. 1159 - 1166 (1990)
Update date:2022-07-29
Topics:
Folkmann
Lund
The synthesis of a number of stable acyloxymethyl carbonochloridates 7 has been accomplished in four steps from chloromethyl carbonochloridate 3. Each step has been optimized with propanoyl-oxymethyl carbonochloridate 7c as a model compound (64% overall yield). Diethyl ether-boron trifluoride catalyzes the conversion of carbonothioate 6cc to the carbonochloridate 7c by chlorination with sulfuryl chloride. Acylation of a few compounds containing hydroxy or amino groups by 7c is described.
View MoreContact:
Address:
Contact:+86-511-88790000
Address:338 North Yushan Rd, Zhenjiang, Jiangsu 212016
Taizhou Green Peptide Trading Co., Ltd.
Contact:13736652831
Address:Room 1501, No71, Yuehe Road, Taizhou City, Zhejiang Province, China
website:https://sdjingyuan.lookchem.com/
Contact:86-531-82687998
Address:Factory Building 11, Jinan Comprehensive free trade zone, Shandong, China
Contact:86-27-84888681
Address:Wuhan economic & technology development zone
Doi:10.1021/acs.orglett.0c03987
(2021)Doi:10.1016/S0040-4039(01)00693-1
(2001)Doi:10.1016/S0040-4020(01)91784-3
(1971)Doi:10.1016/S0040-4039(01)00698-0
(2001)Doi:10.1021/jo00383a005
(1987)Doi:10.1007/BF00945517
()
