Journal of Organic Chemistry p. 2957 - 2959 (1991)
Update date:2022-08-03
Topics:
Stuk, Timothy L.
Grieco, Paul A.
Marsh, Max M.
Oxidation of synthetic manganese(III) porphyrins attached to steroidal substrates at C(17) (cf. 2 and 3) gives rise to hydrogen atom abstraction at C(9) and/or C(12), thereby leading to hydroxyl incorporation at these sites.The use of more robust metalloporphyrins (cf. 9) results in substantial increases in the yields of hydroxylated 5α-androstanes.
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Doi:10.1016/0022-328X(91)83191-6
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