Bulletin of the Chemical Society of Japan p. 2266 - 2269 (1991)
Update date:2022-08-05
Topics:
Akiyama
Takesue
Kumegawa
Nishimoto
Ozaki
5'-O-Acryloyl-5-fluorouridine was preparedd by use of p-methoxybenzyl (PMB) group as an N3-imide protecting group of 5-fluorouridine. PMB group was introduced chemoselectively by use of N,N-diisopropylethylamine or DBU as a base. A new deprotection method was developed by means of AlCl3-anisole system at room temperature.
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