Chemistry of Heterocyclic Compounds p. 623 - 626 (1991)
Update date:2022-08-04
Topics: Yield NMR spectroscopy Chromatography Recrystallization Mass spectrometry (MS) Deprotection TLC (thin-layer chromatography) Protecting group Glycosylation Nucleoside synthesis Solvent system Anomeric Center
Tolstikov, G. A.
Baltina, L. A.
Khalilov, L. M.
Spirikhin, L. V.
Sultanmuratova, V. R.
Murinov, Yu. I.
3-(β-D-Ribofuranosyl)-5-hydroxy-6-methyluracil was synthesized by the silyl method in the presence of SnCl4 using 1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose as the carbohydrate component.The structures of the glycosides were confirmed by spectral methods.
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