SYNTHESIS OF 5-HYDROXY-6-METHYLURACIL 3β-D-RIBOFURANOSIDE

DOI: 10.1007/BF00472512

Source and publish data:

Chemistry of Heterocyclic Compounds p. 623 - 626 (1991)

Update date:2022-08-04

Topics: Yield NMR spectroscopy Chromatography Recrystallization Mass spectrometry (MS) Deprotection TLC (thin-layer chromatography) Protecting group Glycosylation Nucleoside synthesis Solvent system Anomeric Center

Authors:

Tolstikov, G. A.

Baltina, L. A.

Khalilov, L. M.

Spirikhin, L. V.

Sultanmuratova, V. R.

Murinov, Yu. I.

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Article abstract of DOI:10.1007/BF00472512

3-(β-D-Ribofuranosyl)-5-hydroxy-6-methyluracil was synthesized by the silyl method in the presence of SnCl4 using 1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose as the carbohydrate component.The structures of the glycosides were confirmed by spectral methods.

Full text of DOI:10.1007/BF00472512

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