DIAZABICYCLOALKANES WITH BRIDGING NITROGEN ATOMS. 23. SYNTHESIS AND PROPERTIES OF BENZO-1,5-DIAZABICYCLONONEN-3-OL

DOI: 10.1007/BF00476212

Source and publish data:

Chemistry of Heterocyclic Compounds p. 779 - 782 (1991)

Update date:2022-08-04

Topics:

Authors:

Doronina, S. O.

Gall', A. A.

Shishkin, G. V.

Mamatyuk, V. I.

Sal'nikov, G. E.

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Article abstract of DOI:10.1007/BF00476212

Intramolecular cyclization 1-(2-hydrohyethyl)-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-3-ol gives benzo-1,5-diazabicyclo<3.2.2>nonen-3-ols.Further treatment with acetic anhydride gives their 3-acetyl derivatives.The stereoisomers have been separated and their substituent configurations shown by PMR spectroscopy.

Full text of DOI:10.1007/BF00476212

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