Tetrahedron Letters p. 7243 - 7246 (1991)
Update date:2022-08-05
Topics:
Jefford, Charles W.
Jin, Shu-Juan
Bernardinelli, Gerald
1,4-Diphenylcyclopent-2-ene 1,4-endoperoxide on catalysis with trimethylsilyl trifluoromethane-sulfonate reacted with (-)-menthone in a doubly diastereoselective manner to yield two tricyclic 1,2,4-trioxanes having the 3S,5S,6S and 3R,5R,6R configurations respectively. The corresponding pair of 1,3-dioxolanes arising by Baeyer-Villiger-type rearrangement was also formed.
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