Synthesis of bis(pentachlorophenyl)silanediol and related compounds. Crystal structure of diethoxybis(pentachlorophenyl)silane

DOI: 10.1016/0022-328X(92)83111-T

Source and publish data:

Journal of Organometallic Chemistry p. 163 - 171 (1992)

Update date:2022-09-26

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Authors:

Carilla, Jose

Fajari, Lluis

Julia, Luis

Riera, Juan

Lloveras, Joaquin

et al. et al.

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Article abstract of DOI:10.1016/0022-328X(92)83111-T

Bis(pentachlorophenyl) silanediol (3) has been prepared by neutral hydrolysis of perchlorodiphenylsilane (2).Reduction of 2 with LiAlH4 gives bis(pentachlorophenyl)silane (4) which upon treatment with bromine gives dibromobis(pentachlorophenyl)silane (5)

Full text of DOI:10.1016/0022-328X(92)83111-T

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