Synthesis of the Tricyclic Nucleus of the Alkaloid Stemofoline: X-Ray Crystal Structure of (4RS,5RS,7SR,10RS)-10-Butyl-5-hydroxy-1-azatricyclo4,10>decan-2-one

DOI: 10.1039/c39920000538

Source and publish data:

Journal of the Chemical Society. Chemical communications p. 538 - 540 (1992)

Update date:2022-09-26

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Authors:

Beddoes, Roy L.

Davies, Michael P. H.

Thomas, Eric J.

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Article abstract of DOI:10.1039/c39920000538

The tricyclic lactams 20 and 21 have been synthesized using iminium ion cyclisations and formation of the third ring via halogen metal exchange; oxidation of the lactam 22 using lead(IV) acetate gave the tetracyclic ether 27 regioselectively.

Full text of DOI:10.1039/c39920000538

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