Synthesis p. 1235 - 1236 (1992)
Update date:2022-07-29
Topics:
Behrens
Egholm
Buchardt
Selective hydrogenolysis of symmetric bis(hydroxymethyl)aromatic compounds has been performed over Raney nickel in alkaline solution for 24-36 h at 20°C. The yield of the corresponding monohydrogenolysis product was in the range of 75-96%. The usefulness of the reaction was demonstrated by the synthesis of 4-(bromomethyl)benzoic acid.
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