Samarium(II) iodide-mediated reductive cyclization approach to total synthesis of the insect sex attractant (-)-anastrephin

DOI: 10.1016/S0040-4039(00)74773-3

Source and publish data:

Tetrahedron Letters p. 7899 - 7902 (1992)

Update date:2022-09-26

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Authors:

Tadano, Kin-Ichi

Isshiki, Yoshiaki

Minami, Masaki

Ogawa, Seiichiro

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Article abstract of DOI:10.1016/S0040-4039(00)74773-3

Intramolecular reductive cyclization of enantiomerically pure γ,γ-differentially C-substituted α,β-unsaturated ester 5 having a terminal aldehyde functionality, was effectively achieved using SmI₂ in THF-HMPA. Starting with the major cyclizatio

Full text of DOI:10.1016/S0040-4039(00)74773-3

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