A New Phase of Bis<2-(Diphenylphosphino-κP)phenylazanido-κN<(ethanolato)(oxo)rhenium(V)

DOI: 10.1107/S0108270193010029

Source and publish data:

Acta Crystallographica, Section C: Crystal Structure Communications p. 530 - 532 (1994)

Update date:2022-08-03

Topics:

Authors:

Bandoli, Giuliano

Dolmella, Allessandro

Tisato, Francesco

Refosco, Fiorenzo

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Article abstract of DOI:10.1107/S0108270193010029

The title compound, , was synthesized by the oxidation-substitution reaction of III(PNH)2(PNH2)>Cl, where PNH2 is 2-(diphenylphosphino)phenylamine, with NEt3 in EtOH.The X-ray diffraction study of this new triclinic phase, designated β, confirms the molecular structural details for the monoclinic α isomer, which crystalized in space group P2₁/c with a=12.056(3), b=26.303(6), c=11.005(3) Angstroem, β=102.32(2) deg .

Full text of DOI:10.1107/S0108270193010029

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