Scholarly article on H3CC(CH2P(C6H5)H)3 154002-80-9 from Journal of Organometallic Chemistry p. 103 - 106

DOI: 10.1016/S0022-328X(96)06487-X

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Journal of Organometallic Chemistry p. 103 - 106 (1997)

Update date:2022-07-28

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Authors:

Walter, Olaf

Buechner, Michael

Huttner, Gottfried

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Article abstract of DOI:10.1016/S0022-328X(96)06487-X

The tripodal triphosphide H₃CC[CH₂P(Ph)(Li)]₃ reacts with MeSiCl₃ to yield the triphosphinosilane H₃CC[CH₂P(Ph)]₃SiMe, 2a. The analogous reaction with PBr₃ produces the triphosphinophosphine H₃CC[CH₂P(Ph)]₃P, 2b. The bicyclo[2.2.2]octane-type cage structure of 2 is revealed by NMR data as well as X-ray analyses. 2b is one of the rare examples of a compound with mere C₃-symmetry.

Full text of DOI:10.1016/S0022-328X(96)06487-X

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DOI: 10.1016/S0022-328X(96)06487-X