Tetrahedron Letters p. 6733 - 6736 (1994)
Update date:2022-08-03
Topics:
Brown
Brown, Karen M.
Lawrence
Lawrence, Nicholas J.
Liddle
Liddle, John
Muhammad
Muhammad, Faiz
Jackson
Jackson, David A.
A series of substituted benzylphosphine oxides has been synthesized by reduction of the corresponding (α-chlorobenzyl)phosphine oxide, derived from the benzaldehyde and chlorodiphenylphosphine, with either sodium borohydride (DMSO, 60-70 °C, 12 h) or tributyltin hydride and AIBN (C6H6, 80 °C, 2 h). Reaction of the (α-lithiobenzyl)phosphine oxide with aldehydes gave exclusively E-alkenes.
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