Journal of the Chemical Society. Chemical communications p. 833 - 834 (1995)
Update date:2022-08-03
Topics:
Bianchini, Claudio
Cicchi, Stefano
Peruzzini, Maurizio
Pietrusiewicz, K. Michal
Brandi, Alberto
A new approach to the synthesis of chiral P,N-ligands containing a stereogenic phosphorus atom is reported; the synthesis, characterization and coordination properties of (PR,2R,3R,2'R,3'S,4'S) 2<2'(3',4'-di-tert-butoxy-1'-methyltetrahydropyyrolyl)>-3-methoxy-1-phenyltetrahydrophosphole (P*-N-1), which contains a stereogenic phosphorus in addition to five contiguous stereocentres in the ligand backbone; compound P*-N-1 represents the first example of a new class of chiral P,N-ligands with the heteroatoms incorporated in two 2,2'-coupled pyrrolidine-phospholane rings.
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