Tetrahedron Asymmetry p. 1575 - 1583 (1995)
Update date:2022-08-05
Topics:
Nieman
Keay
(±)-cis,cis-2,2'-spirobiindane-1,1'-diol (1) is synthesized stereoselectively in four steps beginning with 1-indanone in 68% overall yield. An improved resolution of diol 1 is described by preparing and separating diastereomeric mono-esters of 1 using (2S)-O-(tert-butyldimethylsilyl)mandeloyl chloride (10).
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Doi:10.1248/cpb.11.1174
(1963)Doi:10.1021/om00010a043
(1995)Doi:10.1021/jm00018a021
(1995)Doi:10.1016/j.bmcl.2005.08.039
(2005)Doi:10.1021/ja00149a024
(1995)Doi:10.1021/jm00021a006
(1995)
