Australian Journal of Chemistry p. 1659 - 1664 (1995)
Update date:2022-07-29
Topics:
Hall, Veronica J.
Tiekink, Edward R. T.
The reaction of Ph3SnCl and Cy2P(O)C(S)N(H)Me yields the air-stable adduct Ph3Sna trigonal bipyramidal tin atom geometry with a chlorine atom a monodentate phosphinyl(thioformamide) ligand, occupying the axial positions.The pale-yellow crystals are monoclinic, space group P21/c with unit cell dimensions a 10.050(1), b 16.501(1), c 19.273(1) Angstroem, β 102.12(1) deg, Z 4; the structure was refined to final R 0.031 by using 5384 reflections.
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