Tetrahedron Letters p. 1889 - 1892 (1996)
Update date:2022-07-31
Topics:
De Mico, Antonella
Margarita, Roberto
Mariani, Andrea
Piancatelli, Giovanni
We describe a new application of iodobenzenediacetate (IBDA), which is able to oxidize thiocyanate anion to the corresponding radical. Subsequent addition to nucleophilic olefins leads to dithiocyanate derivatives. The radical addition to olefins is more effective when performing the thiocyanation reaction in presence of Mg(ClO4)2 or TEMPO.
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(1964)
