Cyclic Metallasiloxane Compounds of Ti(IV) and Zr(IV). X-Ray Crystal Structures of a cis-Bis(pyridine) Bis(cyclosiloxy)titanate and a Pyridinelithiated Tris(cyclosiloxy)zirconate

DOI: 10.1039/DT9890002347

Source and publish data:

Journal of the Chemical Society, Dalton Transactions p. 2347 - 2352 (1989)

Update date:2022-08-03

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Authors:

Hossain, M. Altaf

Hursthouse, Michael B.

Ibrahim, Ali

Mazid, Muhammed

Sullivan, Alice C.

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Article abstract of DOI:10.1039/DT9890002347

The reaction between Si2Ph4O(OLi)2 (1) and TiCl4 in 2:1 or 3:1 molar ratio gave on addition of pyridine (py) the titanatrisiloxane compound 2(py)2>*2C6H5Me (2).Treatment of ZrCl4 with (1) in 1:2 molar ratio gave the zirconadisiloxane

Full text of DOI:10.1039/DT9890002347

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