Tetrahedron Letters p. 3167 - 3170 (1997)
Update date:2022-07-30
Topics:
White, James D.
Ohba, Yoshihiro
Porter, Warren J.
Wang, Shan
A convergent synthesis of the spiroketal subunit of rutamycins A and B has been devised via Julia coupling of sulfone 14 with aldehyde 23; the pentahydroxy ketone 3 derived from 25 underwent spontaneous cyclization to spiroketal 4.
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