Zeitschrift fur Anorganische und Allgemeine Chemie p. 1567 - 1576 (1997)
Update date:2022-08-05
Topics:
M?hlen
Neumüller
Faza
Müller
Massa
Dehnicke
The bromoderivatives of the title compounds are prepared from the corresponding silylated phosphoraneimines Me3SiNPR3 and boron tribromide. The boron subcompound [{B2(NMe2)2.2(NPEt3) 2]Cl2 derives from Me3SiNPEt3 and B2Cl2(NMe2)2. All complexes are characterized by NMR and IR spectroscopy as well as by crystal structure determinations. [BBr2(NPMe3)]2 (1): Space group P21/n, Z = 2, R = 0.031. Lattice dimensions at -50°C: a = 723.8, b = 894.2, c = 1305.4 pm, β = 92.35°. 1 forms centrosymmetric molecules.
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(1968)
