Journal of Organic Chemistry p. 5291 - 5294 (1986)
Update date:2022-09-26
Topics:
Falorni, Massimo
Lardicci, Luciano
Giacomelli, Giampaolo
2,2-Dimethyl-3-(chloromethyl)bicyclo<2.2.1>heptane (camphanyl chloride), camphanyl bromide, 1,7,7-trimethyl-2-(chloromethyl)bicyclo<2.2.1>heptane <2-(chloromethyl)bornane>, and 2-(bromomethyl)bornane were prepared from (+)-camphor.All these compounds were obtained as mixture of exo and endo isomers in various ratios depending upon the synthetic path adopted.A loss of diastereomeric purity during the halogenations of corresponding alcohols was observed.
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