Efficient desilylation of some nucleoside derivatives with potassium tert-butoxide in dimethylformamide

DOI: 10.1080/00397919808004881

Source and publish data:

Synthetic Communications p. 3021 - 3027 (1998)

Update date:2022-08-03

Topics: Yield Purification Workup Reaction Conditions Monitoring Reaction Progress Desilylation Nucleoside derivatives Silyl protecting group Dimethylformamide (DMF)

Authors:

Negron Negron

Vasquez Vasquez

Calderon

Cruz Cruz

Gavino Gavino

Islas Islas

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1080/00397919808004881

A new method for deprotecting silyl ethers of nucleosides has been established by using potassium tert-butoxide in dimethylformamide at room temperature.

Full text of DOI:10.1080/00397919808004881

Synthetic Communications

ISSN: 0039-7911 (Print) 1532-2432 (Online) Journal homepage: http://www.tandfonline.com/loi/lsyc20

Efficient Desilylation of some Nucleoside

Derivatives with Potassium tert-Butoxide in

Dimethylformamide

G. Negrón , F. Vásquezy , G. Calderón , R. Cruz , R. Gaviño & G. Islas

To cite this article: G. Negrón , F. Vásquezy , G. Calderón , R. Cruz , R. Gaviño & G.

Islas (1998) Efficient Desilylation of some Nucleoside Derivatives with Potassium tert-

Butoxide in Dimethylformamide, Synthetic Communications, 28:16, 3021-3027, DOI:

10.1080/00397919808004881

To link to this article: http://dx.doi.org/10.1080/00397919808004881

Published online: 23 Aug 2006.

Submit your article to this journal

Article views: 73

View related articles

Citing articles: 3 View citing articles

Full Terms & Conditions of access and use can be found at

http://www.tandfonline.com/action/journalInformation?journalCode=lsyc20

Download by: [University of Texas Libraries]

Date: 19 May 2016, At: 07:05

Products guided by the article

Product name:Uridine, 5'-O-[(1,1-dimethylethyl)diphenylsilyl]-2',3'-O-(1-methylethylidene)-

Cas No:213552-29-5

R&D Labs maybe for 213552-29-5

shanghai hekang chemical co.ltd

Contact:021-54173790

Address:328 WuHe Road, Building #A, 2nd Floor, Minhang, Shanghai 201109, China
Beijing Zhongshuo Pharmaceutical T & D Co.,Ltd

Contact:0086-10-64430626

Address:ea No 16, HEPINGLI,DONGCHENG DISTRICT,BEIJING,P.R.CHINA.
Shanghai Mintchem Development ., Ltd

Contact:0086 21 5190 8570

Address:R602,4#,89Nong, Mudan Road Pudong Shanghai China
Kunming Biohome Technology Co. Ltd.

website:http://www.biohometech.com/

Contact:86-871-67428869

Address:kunming
BAODING SINO-CHEM INDUSTRY CO.,LTD

Contact:0312-5956088

Address:NO.8 FUXING ROAD,CHINA

Relevant to this article

Doi:10.1007/BF00479580
()
Doi:10.1016/S0040-4039(00)75429-3
(1968)
A Novel NO₂/OH Exchange in α-Nitro Ketones: A Mechanistic Investigation

Doi:10.1002/hlca.19980810547
(1998)
Formal total synthesis of (±)-cortistatin A

Doi:10.1016/j.tet.2010.01.030
(2010)
Reactions of 1-(α-Alkoxyalkyl)- and 1-(α-(Aryloxy)alkyl)benzotriazoles with the Grignard Reagents. A New and Versatile Method for the Preparation of Ethers

Doi:10.1021/jo00287a011
(1989)
The continuous catalytic debenzylation of 1,4-dibenzyloxybenzene with H₂ in THF expanded with high pressure CO₂

Doi:10.1021/op100136g
(2010)

Article Doi