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Stereoselective synthesis and structural establishment of (25S)-24,24- difluoro-1α,25,26-trihydroxyvitamin D3, a major metabolite of 24,24- difluoro-1α,25-dihydroxyvitamin D3

DOI: 10.1016/S0040-4020(98)00949-1

Source and publish data:

Tetrahedron p. 14705 - 14724 (1998)

Update date:2022-09-26

Topics:

Authors:

Iwasaki, HiroshiIwasaki, Hiroshi

Hosotani, RyuzoHosotani, Ryuzo

Miyamoto, YoichiMiyamoto, Yoichi

Nakano, YoshioNakano, Yoshio

Yamamoto, KeikoYamamoto, Keiko

Yamada, SachikoYamada, Sachiko

Shinki, ToshimasaShinki, Toshimasa

Suda, TatsuoSuda, Tatsuo

Yamaguchi, KentaroYamaguchi, Kentaro

Konno, KatsuhiroKonno, Katsuhiro

Takayama, HiroakiTakayama, Hiroaki

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Article abstract of DOI:10.1016/S0040-4020(98)00949-1

(25S)-24,24-Difluoro-1α,25,26-trihydroxyvitamin D3 (3a) and its (25R)- epimer (3b), either of which is expected to be a major metabolite of 24,24- difluoro-1α,25-dihydroxyvitamin D3 (2), were synthesized. Asymmetric addition to β-ket

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Full text of DOI:10.1016/S0040-4020(98)00949-1

Products guided by the article

Product name:(R)-6-{(1R,3aS,7aR)-4-[2-[(3S,5R)-3,5-Bis-(tert-butyl-dimethyl-silanyloxy)-2-methylene-cyclohex-(Z)-ylidene]-eth-(E)-ylidene]-7a-methyl-octahydro-inden-1-yl}-3,3-difluoro-1-((R)-toluene-4-sulfinyl)-heptan-2-one

Cas No:219123-54-3

219123-54-3

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