Chemistry of Heterocyclic Compounds p. 205 - 212 (1992)
Update date:2022-08-05
Topics:
Mikhura, I. V.
Formanovskii, A. A.
A method for the synthesis of aza-crown compounds by the intramolecular cyclization of ω-amino acids with subsequent reduction of the lactam to a macrocyclic amine was developed. 1,8-Diazacyclotetradecane and 1,8-dioxa-4,11-diazacyclotetradecane was synthesized in preparative yields.The structural assignments were made using the IR, 1H and 13C NMR, and mass spectra.
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