Bulletin of the Chemical Society of Japan p. 830 - 832 (1987)
Update date:2022-08-04
Topics:
Tsuboi, Sadao
Ishiguro, Yasuhiro
Takeda, Akira
Electrochemical reduction of exo-5-acetyl-endo-6-trichloromethylbicyclo<2.2.1>hept-2-ene (2) using a mercury cathode gave chemoselectively either the corresponding monochloromethyl or dichloromethyl derivatives in high yields by selecting supporting electrolyte.The reduction of 2 using a lead cathode gave 2-acetyl-3-methylbicyclo<2.2.1>hepta-2,5-diene and cis-1-(4-vinyl-2-cyclopentenyl)-2-propane together wwith by-products.
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