Chemical Communications p. 9507 - 9510 (2015)
Update date:2022-08-03
Topics:
Stephens, David E.
Lakey-Beitia, Johant
Chavez, Gabriel
Ilie, Carla
Arman, Hadi D.
Larionov, Oleg V.
A novel site-selective palladium-catalyzed oxidative C8-H homocoupling reaction of quinoline N-oxides has been developed. The reaction affords substituted 8,8′-biquinolyl N,N′-dioxides that can be readily converted to a variety of functionalized 8,8′-biquinolyls. Mechanistic studies point to the crucial role of the oxidant and a non-innocent behavior of acetic acid as a solvent.
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