European Journal of Organic Chemistry p. 3022 - 3034 (2019)
Update date:2022-08-05
Fernandes, Alessandra A. G.
da Silva, Amanda F.
Okada, Celso Y.
Suzukawa, Vitor
Cormanich, Rodrigo A.
Jurberg, Igor D.
A general platform for the conversion of isoxazol-5-ones to 3,5-disubstituted isoxazoles has been developed via a two-step strategy. The first step leads to the formation of 5-(pseudo)halogenated isoxazoles, while in the second, a variety of heteroalkyl-, heteroaryl-, alkyl-, alkenyl-, alkynyl- and aryl-chains can be installed via nucleophilic substitutions or palladium catalyzed cross-coupling reactions.
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