Generation and C-Ethoxycarbonylation of Enolates Using Ultrasound

DOI: 10.1246/cl.1986.1251

Source and publish data:

Chemistry Letters p. 1251 - 1254 (1986)

Update date:2022-07-29

Topics:

Authors:

Palominos, Mario A.

Rodriguez, Robinson

Vega, Juan C.

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Article abstract of DOI:10.1246/cl.1986.1251

O-Ethyl 3-oxothioesters were obtained in good yields by reaction of O,O-diethyl trithiodicarbonate with enolate from ketones and NaH in tetrahydrofuran.The enolate formation and thioacylation were performed under ultrasonic irradiation.

Full text of DOI:10.1246/cl.1986.1251

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