Generation and C-Ethoxycarbonylation of Enolates Using Ultrasound

DOI: 10.1246/cl.1986.1251

Source and publish data:

Chemistry Letters p. 1251 - 1254 (1986)

Update date:2022-07-29

Topics:

Authors:

Palominos, Mario A.

Rodriguez, Robinson

Vega, Juan C.

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1246/cl.1986.1251

O-Ethyl 3-oxothioesters were obtained in good yields by reaction of O,O-diethyl trithiodicarbonate with enolate from ketones and NaH in tetrahydrofuran.The enolate formation and thioacylation were performed under ultrasonic irradiation.

Full text of DOI:10.1246/cl.1986.1251

Products guided by the article

Product name:Cyclohexanecarbothioic acid, 2-oxo-, O-ethyl ester

Cas No:41500-03-2

R&D Labs maybe for 41500-03-2

AURORA CHEMICAL CO., LTD

Contact:86-532-68629711 13780605697

Address:NO 220 YANAN 3 ROAD,(POST ADMINISTRATION BUILDING),QINGDAO,CHINA
Anhui Jiatiansen Agrochemical Co.,Ltd

Contact:15366811918

Address:chemical industrial park,xiangyu town,dongzhi county,anhui,china
Qingdao S. H. Huanyu Imp. & Exp. Co., Ltd.

Contact:86-532-88250866

Address:Room 615, World Trade Centre Building B, Hongkong Middle Roda 6#, Qingdao, Shandong, China
SHIJIAZHUANG HENRYTE CHEMICALS CO,.LTD(expird)

Contact:+86-311-85208698 311-80837698

Address:NO.166, yuhua west road, SHIJIAZHUANG, China
KindChem Co.,Ltd,

Contact:+86-25-85281586

Address:13F,Bld2#,South of Longpan Road

Relevant to this article

Photoelimination of nitrogen from adamantane and pentacycloundecane (PCU) diazirines: A spectroscopic study and supramolecular control

Doi:10.1039/c9pp00124g
(2019)
Synthesis of some new tetrahydrobenzo[b] thiophene derivatives and tetrahydrobenzo-thienopyrimidine derivatives under microwave irradiation

Doi:10.1080/00397911.2010.501479
(2011)
Doi:10.1016/S0022-328X(00)84996-7
(1973)
Conceptually new low-calcemic oxime analogues of the hormone 1α,25-dihydroxyvitamin D₃: Synthesis and biological testing

Doi:10.1021/jm010560o
(2002)
Evidence supporting the formation of 2,3-epoxy-3-methylindoline: A reactive intermediate of the pneumotoxin 3-methylindole

Doi:10.1021/tx9702087
(1998)
Visible-light-mediated deuteration of aldehydes with D₂O via polarity-matched reversible hydrogen atom transfer

Doi:10.1016/j.tet.2021.131946
(2021)

Article Doi