Tetrahedron Letters p. 6901 - 6902 (1998)
Update date:2022-08-04
Topics:
Miyano, Akira
Tashiro, Daisuke
Kawasaki, Yumi
Sakaguchi, Satoshi
Ishii, Yasutaka
Aliphatic aldehydes underwent trimerization in the presence of a catalytic amount of Cp*2Sm(thf)2 under ambient conditions to form 1,3- diol monoestcrs in good yields. For example, the reaction of acetoaldehyde catalyzed by Cp*2Sm(thf)2 gave 4-acetoxy-2-butanol (2a) and 3-acetoxy-1- butanol (3a) in 86% yield.
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Doi:10.1016/S0040-4020(98)00831-X
(1998)Doi:10.1016/j.tet.2018.09.054
(2018)Doi:10.1039/jr9490000842
(1949)Doi:10.1021/jacs.5b02537
(2015)Doi:10.1002/jps.2600640430
(1975)Doi:10.1007/BF01175082
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