Tetrahedron p. 1631 - 1636 (1988)
Update date:2022-08-03
Topics: NMR spectroscopy Product Isolation Cyclic Voltammetry (CV) Electrolyte Anode Cathode Electrochemical Reduction Carboxylation Electrosynthesis Faradaic Efficiency Working electrode Reference electrode Counter electrode
Heintz, Monique
Sock, Oumar
Saboureau, Christophe
Perichon, Jacques
Troupel, Michel
The electrocarboxylation of a large variety of chlorobenzenic compounds is achieved in N,N-dimethylformamide by constant current electrolysis between a stainless steel cathode and a sacrificial magnesium anode in a diaphragmless cell. Substituted benzoic acids are obtained in high yield in simle conditions thus avoiding the usual preparation of organometallic intermediates.
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