Exclusive formation of crystalline sp-9-(o-isopropylphenyl)fluorene from its ap rotamer in solution

DOI: 10.1107/S0108270197003739

Source and publish data:

Acta Crystallographica, Section C: Crystal Structure Communications p. 1149 - 1151 (1997)

Update date:2022-08-05

Topics:

Authors:

Meyers, Cal Y.

Hou, Yuqing

Scott, Delano

Robinson, Paul D.

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Article abstract of DOI:10.1107/S0108270197003739

Reduction of ap-9-(o-isopropylphenyl)-9-fluorenol provided 9-(o-isopropylphenyl)fluorene shown to be the sp and ap rotamers in solution by ¹H NMR. Evaporation of the solvent yielded sharp-melting crystals identified by X-ray diffraction as sp-9

Full text of DOI:10.1107/S0108270197003739

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