Research on Chemical Intermediates p. 101 - 110 (2013)
Update date:2022-07-30
Topics:
Yanagisawa, Yuuki
Yamaguchi, Hiroki
Nishiyama, Yasuhiro
Morimoto, Tsumoru
Kakiuchi, Kiyomi
Tabata, Kenji
Tsutsumi, Ken
A novel chiral menthol derivative supported on silsesquioxane was easily synthesized by hydrosilylation of the corresponding arylmenthyl olefin with commercially available silsesquioxane-type hydrosilane. We evaluated the applicability of the silsesquioxane-based compound to diastereoselective [2+2] photocycloaddition reaction. The newly synthesized silsesquioxane-based chiral menthol derivative 9 indicated similar diastereoselectivity to the corresponding p-methoxyphenyl menthol derivative.
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