Russian Chemical Bulletin p. 378 - 380 (2000)
Update date:2022-07-30
Topics:
Epstein
Savchenko
Kulinkovich
The reaction of (CD3)2CHMgBr with ethyl 3-chloropropionate in the presence of catalytic amounts of Ti(OPr1)4 results in (E)-1-(2-chloroethyl)-3,3-dideuterio-2-trideuteriomethylcyclopropanol and (CD3)2CDH, identified by mass spectrometry. The reaction mechanism is discussed.
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