Cyclization of Dinitrophenyl tert-Butyl Trithiocarbonates. A Novel Synthesis of Nitro-1,3-benzodithiole-2-thiones

DOI: 10.1021/jo01308a020

Source and publish data:

Journal of Organic Chemistry p. 4041 - 4044 (1980)

Update date:2022-08-02

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Authors:

Rasheed, Khalid

Warkentin, James D.

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Article abstract of DOI:10.1021/jo01308a020

Reaction of the sodium salt of tert-butyl trithiocarbonic acid with chlorodinitrobenzenes yields dinitrophenyl tert-butyl trithiocarbonates.The latter cyclize on heating in glacial acetic acid to nitro-1,3-benzodithiole-2-thiones.

Full text of DOI:10.1021/jo01308a020

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