The Reaction of 2-(Trialkylsiloxy)furans with Lead(IV) Acetate. The Synthesis of dl-Pyrenophorin

DOI: 10.1246/bcsj.53.1061

Source and publish data:

Bulletin of the Chemical Society of Japan p. 1061 - 1064 (1980)

Update date:2022-08-04

Topics:

Authors:

Asaoka, Morio

Yanagida, Noboru

Sugimura, Naoyuki

Takei, Hisashi

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1246/bcsj.53.1061

The reaction of 2-(trimethylsiloxy)furans with lead(IV) acetate afforded the corresponding α,β-unsaturated γ-acetoxy-γ-lactones in good yields.The lactones were easily converted into the corresponding 3-acylacrylic acids.Utilizing this reaction, dl-pyrenophorin was synthesized.

Full text of DOI:10.1246/bcsj.53.1061

Products guided by the article

Product name:2(5H)-Furanone, 5-(3-oxobutyl)-

Cas No:74982-60-8

R&D Labs maybe for 74982-60-8

ShangHai Ruiyi Medical Technology Co.,Ltd.

Contact:+86-21-54718086

Address:No951 Jianchuan RD，Minhang District
Chengdu NoVi Biotechnology Co., Ltd.(expird)

Contact:13551243286/028-81458053

Address:NO.168-1-224 JULONG ROAD WUHOU DISTRICT, CHENGDU CITY,SICHUAN PROVINCE
Tianjin Pharmacn Medical Technology Co.,Ltd.

Contact:86-22-60122566ext.866(English),23359620

Address:Green Industrial Base, 6 Haitaifazhan Sixth Rd., Huayuan Industrial Area, Tianjin, 300384, China
Jiangsu Cale New Material Co.ltd

Contact:+86-515-88334667/88203550

Address:Zhongshan 3rd Road, Coastal Chemical Industry Park, Yancheng, Jiangsu, China
Shanghai Ingredients Technology Co., Ltd.(expird)

website:http://www.jiahealthy.com

Contact:0086-21-6174 0809

Address:20F, No 1018 ChangNing Road, Shanghai City

Relevant to this article

Studies on heterocyclic compounds; III. Synthesis of benzo[g]thieno[2,3-a]quinolizines

Doi:10.1055/s-1980-29057
(1980)
Dithiocarbamate group transfer cyclization reactions of carbamoyl radicals under "tin-free" conditions

Doi:10.1002/anie.200453600
(2004)
Synthesis and biological evaluation of analogues of the marine cyclic depsipeptide obyanamide

Doi:10.1002/psc.1361
(2011)
Antihypertensive (2-Aminoethyl)thiourea Derivatives. 1

Doi:10.1021/jm00186a019
(1980)
Doi:10.1039/c19660000577
(1966)
Reaction between ^tBuMgCl and SnCl₄, illustrating the solvent-dependent predominant formation of Cl(^tBu₂Sn) _nCl (THF, n = 1; Toluene, n = 2; Hexane, n = 3) and the subsequent wavelength-selective photochemical transformation of n = 3 → 2 → 1

Doi:10.1021/om200548s
(2011)

Article Doi