Tetrahedron p. 1859 - 1872 (1986)
Update date:2022-07-30
Topics:
Kiggen, W.
Voegtle, F.
Franken, S.
Puff, H.
The syntheses of oligocyclic large cavities containing two or three catechol subunits are described.The X-ray analysis of a heptacyclic molecule composed of three triply clamped dimethyl catechol ether units demonstrates the size and shape of the cavity formed by this skeleton.Properties of the Fe(3+)- and Ga(3+)-complexes are elucidated by (1)H-NMR, IR, UV/Vis spectra, and by competition experiments with an open-chained reference ligand.
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