Synthesis p. 1747 - 1749 (2004)
Update date:2022-08-02
Topics:
Akhlaghinia, Batool
Pourali, Ali Reza
Alkyl nitrites were prepared in good to excellent yields by treatment of alcohols and thiols with triphenylphosphine/2,3-dichloro-5,6- dicyanobenzoquinone/Bu4NNO2 in acetonitrile. This method is highly selective for the conversion of primary alcohols to alkyl nitrites in the presence of secondary and tertiary alcohols and thiols.
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(2004)
