Journal of Organic Chemistry p. 2697 - 2700 (1982)
Update date:2022-08-03
Topics:
Kita, Yasuyuki
Haruta, Jun-ichi
Yasuda, Hitoshi
Fukunaga, Keiko
Shirouchi, Yoshiaki
Tamura, Yasumitsu
A new method for the preparation of tert-butyl- (1d), benzyl- (1e), and (β-trimethylsilyl)ethyl α-methoxyvinyl carbonates (1f) has been devised.The reaction of these reagents with amino compounds proceeds rapidly under mild conditions to give the corresponding N-tert-butoxycarbonylated (N-Boc), N-benzyloxycarbonylated (N-Z), and N-<β-(trimethylsilyl)ethoxy>carbonylated (N-Tmseoc) compounds in quantitative yields.Twenty-two examples using amines, amino alcohols, and amino acids were presented.
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Doi:10.1021/acs.jafc.6b02390
(2016)Doi:10.1002/ardp.19823150412
(1982)Doi:10.1021/ja00543a012
(1980)Doi:10.1055/s-1986-31848
(1986)Doi:10.1039/P19820000741
(1982)Doi:10.1016/0008-6215(82)85034-9
(1982)
