Chemistry Letters p. 593 - 596 (1982)
Update date:2022-09-26
Topics:
Takeda, Takeshi
Furukawa, Hiroyuki
Fujiwara, Tooru
1-(Methylthio) and 1-(phenylthio)vinyllithiums were prepared by the treatment of the corresponding 2-methoxyethyl sulfides with twice molar amounts of butyllithium in the presence of N,N,N',N'-tetramethylethylenediamine (TMEDA). β-Alkylthio-β,γ-unsaturated alcohols were obtained in good yields by the reaction of the lithium salts with aldehydes.
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