Journal of Organometallic Chemistry p. 161 - 166 (1984)
Update date:2022-08-04
Topics:
Grant, Douglas W.
Wardell, James L.
The Sn-Se bond in trimethyltin aryl selenides is cleaved on reaction with selenenyl halides, sulphenyl halides, alkyl halides and allyl halides.Thus Me3SnSePh reacts with PhSeCl, 4-Me-2-NO2C6H3SCl, RI (R = CH3 or Ph3SnCH2) and CH2=CHCH2Br to give PhSeSePh, 4-Me-2-NO2C6H3SSePh, RSePh and CH2=CHCH2SePh, respectively.The diselenide, PhSeSePh, is also obtained from Me3SnSePh on reaction with either 4-MeC6H4SO2Cl or NaIO4.Exchange reactions also occur between Me3SnSePh and Ph3SnCl or PhHgCl.
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